$crystalmaker electron diffraction pattern example$

$crystalmaker electron diffraction pattern example$

With theophylline, we identify crystals of “impurity” polymorphic phases in samples that appear from powder X‐ray diffraction to be monophasic, and observe that crystal growth behavior of samples prepared from nitromethane is significantly different to that of samples prepared from methanol. A range of relevant information about these compounds is derived including morphology, polymorph identification, mapping of crystal habit to crystal structure and crystal defect characterization.

$crystalmaker electron diffraction pattern example$

In this overview, we describe straightforward approaches for overcoming these issues which have enabled us to characterize a variety of pharmaceutical compounds, including theophylline, paracetamol and aspirin, and also pharmaceutical salts and cocrystals. Its use for characterization of pharmaceutical samples has, however, been very limited, largely due to the difficulties associated with the preparation of appropriately thin samples, as well as issues with sample damage caused by the electron beam. Transmission electron microscopy (TEM) and its facility for electron diffraction has long been a key technique in materials science. Transmission electron microscopy of pharmaceutical materials Transmission electron microscopy of pharmaceutical materialsĮddleston, Mark D.

$crystalmaker electron diffraction pattern example$

Crystalmaker electron diffraction pattern example